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AbstractInfrared IR absorption spectra of melamine-formaldehyde (MF) microparticles confined in an rf plasma are studied at different plasma conditions. Several absorption peaks have been analysed in dependence of plasma power and their temporal evolution. For comparison, the IR absorption spectra of heated MF microparticles without plasma exposition are used to determine the general influence of the temperature on the IR spectra. Measuring the temperature of the particles inside the plasma shows that the temperature is not the only process changing the particles’ IR spectra. Chemical changes of the MF particles with increasing plasma power influence the absorption peak structure.